CN106305825A - Traditional Chinese medicine pesticide and preparation method thereof - Google Patents

Traditional Chinese medicine pesticide and preparation method thereof Download PDF

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CN106305825A
CN106305825A CN201610673506.8A CN201610673506A CN106305825A CN 106305825 A CN106305825 A CN 106305825A CN 201610673506 A CN201610673506 A CN 201610673506A CN 106305825 A CN106305825 A CN 106305825A
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chinese medicine
traditional chinese
pesticide
powder
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邓新平
聂雄
黄庭宝
傅小妮
李小周
卢煜海
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Guangxi University
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/02Sulfur; Selenium; Tellurium; Compounds thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/16Heavy metals; Compounds thereof
    • A01N59/22Arsenic
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N63/00Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
    • A01N63/10Animals; Substances produced thereby or obtained therefrom
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N63/00Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
    • A01N63/30Microbial fungi; Substances produced thereby or obtained therefrom
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/38Solanaceae [Potato family], e.g. nightshade, tomato, tobacco or chilli pepper

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  • Life Sciences & Earth Sciences (AREA)
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  • General Health & Medical Sciences (AREA)
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  • Inorganic Chemistry (AREA)
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Abstract

本发明属于农药制剂研发技术领域,特别涉及一种中药农药及其制备方法。一种中药农药,由按重量份比的以下原料制成:使君子50‑70份、桑叶20‑40份、岗松25‑35份、臭椿叶15‑25份、朴硝20‑35份、大叶桉25‑35份、满山香20‑30份、洋金花5‑20份、雄黄粉5‑15份、五倍子15‑25份、黑牵牛15‑25份、鱼腥草15‑30份和雷丸15‑30份。本发明的中药农药主要成分为天然中药原料,配比合理,原料间协同增效,药液在农作物中残留时间短,能在土壤中自动转化成肥料;本发明的中药农药环保、健康、使用简单、方便,具有低毒、安全、成本低廉的特点;本发明的中药农药对农作物具有良好的杀虫、驱虫、杀菌效果,且能够防病、治病,适用范围广。The invention belongs to the technical field of research and development of pesticide preparations, in particular to a traditional Chinese medicine pesticide and a preparation method thereof. A traditional Chinese medicine pesticide, which is made from the following raw materials in parts by weight: 50-70 parts of Shijunzi, 20-40 parts of mulberry leaves, 25-35 parts of Gangsong pine, 15-25 parts of Ailanthus leaves, 20-35 parts of Pu Nitrate, 25-35 parts of Eucalyptus eucalyptus, 20-30 parts of Manshanxiang, 5-20 parts of Yangjinhua, 5-15 parts of realgar powder, 15-25 parts of Chinese gall, 15-25 parts of black petunia, 15-30 parts of Houttuynia cordata 15‑30 parts and Lei Wan. The main component of the traditional Chinese medicine pesticide of the present invention is natural traditional Chinese medicine raw materials, the proportioning is reasonable, the raw materials are synergistically synergistic, the liquid medicine remains in crops for a short time, and can be automatically converted into fertilizer in the soil; the traditional Chinese medicine pesticide of the present invention is environmentally friendly, healthy and easy to use The invention is simple and convenient, has the characteristics of low toxicity, safety and low cost; the traditional Chinese medicine pesticide of the invention has good insecticidal, anthelmintic and bactericidal effects on crops, can prevent and cure diseases, and has a wide range of applications.

Description

一种中药农药及其制备方法A kind of traditional Chinese medicine pesticide and preparation method thereof

技术领域technical field

本发明属于农药制剂研发技术领域,特别涉及一种中药农药及其制备方法。The invention belongs to the technical field of research and development of pesticide preparations, in particular to a traditional Chinese medicine pesticide and a preparation method thereof.

背景技术Background technique

在传统观念中,中草药主要用于人体或动物体的疾病治疗与保健,将中草药制成农药作用于植物体的相关报道较少。在目前的农业生产中,化学农药的普遍使用有效地遏制了农作物病虫害,但是同时也给人畜以及整个生态环境造成了严重污染。通常使用的化学农药毒性大,在农作物中会有一定的残留,对人类健康存在潜在的威胁。突破桎梏,采用中药原料制备一种农药,该药物成分来源于可供人体内服或外用的天然植物,是新农业开发的一种需要。In the traditional concept, Chinese herbal medicines are mainly used for the treatment and health care of human or animal diseases, and there are few reports about making Chinese herbal medicines into pesticides and acting on plants. In the current agricultural production, the widespread use of chemical pesticides has effectively curbed crop diseases and insect pests, but at the same time it has also caused serious pollution to humans, animals and the entire ecological environment. The commonly used chemical pesticides are highly toxic and will have certain residues in crops, posing a potential threat to human health. Breaking through the shackles, using traditional Chinese medicine raw materials to prepare a pesticide, the medicinal ingredients are derived from natural plants that can be taken internally or externally by the human body, which is a need for the development of new agriculture.

公开于该背景技术部分的信息仅仅旨在增加对本发明的总体背景的理解,而不应当被视为承认或以任何形式暗示该信息构成已为本领域一般技术人员所公知的现有技术。The information disclosed in this Background section is only for enhancing the understanding of the general background of the present invention and should not be taken as an acknowledgment or any form of suggestion that the information constitutes the prior art that is already known to those skilled in the art.

发明内容Contents of the invention

针对现有技术中存在的上述不足,本发明所要解决的技术问题之一提供一种中药农药及其制备方法。Aiming at the above-mentioned deficiencies in the prior art, one of the technical problems to be solved by the present invention is to provide a traditional Chinese medicine pesticide and a preparation method thereof.

为了实现上述目的,本发明是采用以下技术方案实现:In order to achieve the above object, the present invention adopts the following technical solutions to realize:

一种中药农药,由按重量份比的以下原料制成:使君子50-70份、桑叶20-40份、岗松25-35份、臭椿叶15-25份、朴硝20-35份、大叶桉25-35份、满山香20-30份、洋金花5-20份、雄黄粉5-15份、五倍子15-25份、黑牵牛15-25份、鱼腥草15-30份和雷丸15-30份。A traditional Chinese medicine pesticide, which is made from the following raw materials in proportion by weight: 50-70 parts of Shijunzi, 20-40 parts of mulberry leaves, 25-35 parts of Gangsong pine, 15-25 parts of Ailanthus ailanthii leaves, 20-35 parts of Pu Nitrate, 25-35 parts of Eucalyptus eucalyptus, 20-30 parts of Manshanxiang, 5-20 parts of Yangjinhua, 5-15 parts of realgar powder, 15-25 parts of gallnut, 15-25 parts of black petunia, 15-30 parts of Houttuynia cordata 15-30 parts and Lei Wan.

作为优选,所述的中药农药,由按重量份比的以下原料制成:使君子65份、桑叶30份、岗松30份、臭椿叶20份、朴硝30份、大叶桉30份、满山香25份、洋金花19份、雄黄粉13份、五倍子20份、黑牵牛20份、鱼腥草25份和雷丸25份。As preferably, the described traditional Chinese medicine pesticide is made from the following raw materials in parts by weight: 65 parts of Gentleman, 30 parts of mulberry leaves, 30 parts of Pinus pine, 20 parts of Ailanthus leaves, 30 parts of Pu Nitrate, 30 parts of Eucalyptus eucalyptus, Manshanxiang 25 parts, Yangjinhua 19 parts, realgar powder 13 parts, gallnut 20 parts, black petunia 20 parts, Houttuynia cordata 25 parts and Leiwan 25 parts.

此外,本发明还提供了所述的中药农药的制备方法,包括以下步骤:In addition, the present invention also provides a preparation method of the traditional Chinese medicine pesticide, comprising the following steps:

(1)按重量份数称取以上各中药原料,将雷丸干燥,打成细粉,得雷丸粉;(1) take above each Chinese medicine raw material by parts by weight, dry Lei Wan, beat into fine powder, obtain Lei Wan powder;

(2)将使君子、桑叶、岗松、臭椿叶、大叶桉、满山香、洋金花、五倍子、黑牵牛、鱼腥草10种中药置入大瓦锅内,加入自来水,浸泡8-10h后,用武火烧开,再用文火熬煮60-90min后,过滤,将药液和药渣分离,得第一次煎煮液;(2) Put 10 kinds of traditional Chinese medicines such as Shijunzi, mulberry leaves, pine pines, Ailanthus leaves, Eucalyptus euphratica, Manshanxiang, Yangjinhua, gallnut, petunias, and Houttuynia cordata into a large earthenware pot, add tap water, and soak After 8-10 hours, bring to a boil with strong fire, then boil with slow fire for 60-90 minutes, filter, separate the medicinal liquid and medicinal residues, and obtain the first decoction liquid;

(3)然后往药渣中再加入自来水,用武火烧开,再用文火熬煮60-120min后关火倒出,得第二次煎煮液;(3) Then add tap water to the medicinal dregs, bring to a boil with strong fire, boil with slow fire for 60-120 minutes, turn off the fire and pour it out to obtain the second decoction;

(4)把步骤(2)所得的第一次煎煮液和步骤(3)所得的第二次煎煮液合并,过滤,浓缩,得到浓缩药液;(4) combining the first decoction liquid obtained in step (2) and the second decoction liquid obtained in step (3), filtering, and concentrating to obtain concentrated medicinal liquid;

(5)再把朴硝、雄黄粉及步骤(1)所得雷丸粉倒进浓缩药液中,搅拌均匀,即得本发明中药农药。(5) Pour the salted salt, realgar powder and thunder pill powder obtained in step (1) into the concentrated medicinal liquid, and stir evenly to obtain the traditional Chinese medicine pesticide of the present invention.

作为优选,步骤(1)中雷丸粉的细度为100-200目。As preferably, the fineness of the thunder ball powder in the step (1) is 100-200 mesh.

作为优选,步骤(2)中自来水的加入量为10种中药重量的15-20倍。As preferably, the addition of tap water in the step (2) is 15-20 times of the weight of 10 kinds of traditional Chinese medicines.

作为优选,步骤(3)中自来水的加入量为药渣重量的5-10倍。As preferably, the addition of tap water in step (3) is 5-10 times of the weight of medicinal residues.

作为优选,步骤(4)中浓缩药液的密度为1.0-1.5g/cm3。Preferably, the density of the concentrated medicinal solution in step (4) is 1.0-1.5 g/cm3.

本发明还提供了所述的中药农药使用方法:将本发明中药农药与水按10:100的比例进行稀释,得到稀释液,然后直接将稀释液均匀喷施到农作物叶面上,每隔3-4天喷施1次,连续喷施2-3次,每亩用50kg稀释液,即可达到防治病虫害的目的。The present invention also provides the method for using the traditional Chinese medicine pesticide: dilute the traditional Chinese medicine pesticide of the present invention with water at a ratio of 10:100 to obtain a diluted solution, and then directly spray the diluted solution evenly on the leaves of the crops, every 3 -Spray once every 4 days, spray 2-3 times continuously, and use 50kg dilution per mu to achieve the purpose of preventing and controlling pests and diseases.

本发明适用于小麦、玉米、花生、水稻、水果、蔬菜等农作物病虫害的防治。The invention is applicable to the prevention and control of crop diseases and insect pests such as wheat, corn, peanuts, rice, fruits and vegetables.

与现有技术相比,本发明具有如下有益效果:Compared with the prior art, the present invention has the following beneficial effects:

(1)本发明的中药农药主要成分为天然中药原料,配比合理,原料间协同增效,药液在农作物中残留时间短,能在土壤中自动转化成肥料。(1) The main components of the traditional Chinese medicine pesticide of the present invention are natural traditional Chinese medicine raw materials, the proportioning ratio is reasonable, the raw materials are synergistic, the medicinal liquid has a short residual time in the crops, and can be automatically converted into fertilizer in the soil.

(2)本发明的中药农药环保、健康、使用简单、方便,具有低毒、安全、成本低廉的特点。(2) The traditional Chinese medicine pesticide of the present invention is environmentally friendly, healthy, simple and convenient to use, and has the characteristics of low toxicity, safety and low cost.

(3)本发明的中药农药对农作物具有良好的杀虫、驱虫、杀菌效果,且能够防病、治病,适用范围广。(3) The traditional Chinese medicine pesticide of the present invention has good insecticidal, anthelmintic, and bactericidal effects on crops, and can prevent and cure diseases, and has a wide range of applications.

(4)本发明的中药农药的制备方法简单易操作,具有良好的推广和应用前景。(4) The preparation method of the traditional Chinese medicine pesticide of the present invention is simple and easy to operate, and has good promotion and application prospects.

具体实施方式detailed description

下面结合具体实施例对本发明的具体实施方式进行详细描述,但应当理解本发明的保护范围并不受具体实施方式的限制。The specific embodiments of the present invention will be described in detail below in conjunction with specific examples, but it should be understood that the protection scope of the present invention is not limited by the specific embodiments.

实施例1 Embodiment 1 :

一种中药农药,由按重量份比的以下原料制成:使君子50份、桑叶20份、岗松25份、臭椿叶15份、朴硝20份、大叶桉25份、满山香20份、洋金花5份、雄黄粉5份、五倍子15份、黑牵牛15份、鱼腥草15份和雷丸15份。A traditional Chinese medicine pesticide, which is prepared from the following raw materials in proportion by weight: 50 parts of Gentleman, 20 parts of mulberry leaves, 25 parts of Gangsong pine, 15 parts of Ailanthus ailanthus leaves, 20 parts of Pu Nitrate, 25 parts of Eucalyptus eucalyptus, 20 parts of Manshanxiang , 5 parts of Dajinhua, 5 parts of realgar powder, 15 parts of gallnut, 15 parts of black petunia, 15 parts of Houttuynia cordata and 15 parts of Lei Wan.

所述的中药农药的制备方法,包括以下步骤:The preparation method of described traditional Chinese medicine pesticide, comprises the following steps:

(1)按重量份数称取以上各中药原料,将雷丸干燥,打成细粉,得雷丸粉;雷丸粉的细度为100-200目;(1) take above each Chinese medicine raw material by parts by weight, dry the thunder pill, beat into fine powder, obtain the thunder pill powder; the fineness of the thunder pill powder is 100-200 order;

(2)将使君子、桑叶、岗松、臭椿叶、大叶桉、满山香、洋金花、五倍子、黑牵牛、鱼腥草10种中药置入大瓦锅内,加入自来水,浸泡8h后,用武火烧开,再用文火熬煮60min后,过滤,将药液和药渣分离,得第一次煎煮液;自来水的加入量为10种中药重量的15倍;(2) Put 10 kinds of traditional Chinese medicines such as Shijunzi, mulberry leaves, pine pines, Ailanthus leaves, Eucalyptus euphratica, Manshanxiang, Yangjinhua, gallnut, petunias, and Houttuynia cordata into a large earthenware pot, add tap water, and soak After 8 hours, bring to a boil with a strong fire, then boil with a slow fire for 60 minutes, filter, separate the medicinal liquid and medicinal residues, and obtain the first decoction liquid; the amount of tap water added is 15 times the weight of 10 kinds of traditional Chinese medicines;

(3)然后往药渣中再加入自来水,用武火烧开,再用文火熬煮60min后关火倒出,得第二次煎煮液;自来水的加入量为药渣重量的5倍;(3) Then add tap water to the medicinal dregs, bring to a boil with strong fire, then turn off the fire and pour it out after simmering for 60 minutes to obtain the second decoction; the amount of tap water added is 5 times the weight of medicinal dregs;

(4)把步骤(2)所得的第一次煎煮液和步骤(3)所得的第二次煎煮液合并,过滤,浓缩,得到浓缩药液;浓缩药液的密度为1.0g/cm3(4) The first decoction liquid of step (2) gained and the second decoction liquid of step (3) gained are combined, filtered and concentrated to obtain concentrated medicinal liquid; the density of concentrated medicinal liquid is 1.0g/cm 3 ;

(5)再把朴硝、雄黄粉及步骤(1)所得雷丸粉倒进浓缩药液中,搅拌均匀,即得本发明中药农药。(5) Pour the salted salt, realgar powder and thunder pill powder obtained in step (1) into the concentrated medicinal liquid, and stir evenly to obtain the traditional Chinese medicine pesticide of the present invention.

实施例2 Embodiment 2 :

一种中药农药,由按重量份比的以下原料制成:使君子70份、桑叶40份、岗松35份、臭椿叶25份、朴硝35份、大叶桉35份、满山香30份、洋金花20份、雄黄粉15份、五倍子25份、黑牵牛25份、鱼腥草30份和雷丸30份。A traditional Chinese medicine pesticide, which is prepared from the following raw materials by weight: 70 parts of Gentleman, 40 parts of mulberry leaves, 35 parts of Gangsong pine, 25 parts of Ailanthus ailanthus leaves, 35 parts of Pu Nitrate, 35 parts of Eucalyptus eucalyptus, and 30 parts of Manshanxiang , 20 parts of Yangjinhua, 15 parts of realgar powder, 25 parts of gallnut, 25 parts of black petunia, 30 parts of Houttuynia cordata and 30 parts of Lei Wan.

所述的中药农药的制备方法,包括以下步骤:The preparation method of described traditional Chinese medicine pesticide, comprises the following steps:

(1)按重量份数称取以上各中药原料,将雷丸干燥,打成细粉,得雷丸粉;雷丸粉的细度为200目;(1) take above each Chinese medicine raw material by parts by weight, dry the thunder pill, beat into fine powder, obtain the thunder pill powder; the fineness of the thunder pill powder is 200 orders;

(2)将使君子、桑叶、岗松、臭椿叶、大叶桉、满山香、洋金花、五倍子、黑牵牛、鱼腥草10种中药置入大瓦锅内,加入自来水,浸泡10h后,用武火烧开,再用文火熬煮90min后,过滤,将药液和药渣分离,得第一次煎煮液;自来水的加入量为10种中药重量的20倍;(2) Put 10 kinds of traditional Chinese medicines such as Shijunzi, mulberry leaves, pine pines, Ailanthus leaves, Eucalyptus euphratica, Manshanxiang, Yangjinhua, gallnut, petunias, and Houttuynia cordata into a large earthenware pot, add tap water, and soak After 10 hours, bring to a boil with a strong fire, then boil with a slow fire for 90 minutes, filter, separate the medicinal liquid and medicinal residues, and obtain the first decoction liquid; the amount of tap water added is 20 times the weight of 10 kinds of traditional Chinese medicines;

(3)然后往药渣中再加入自来水,用武火烧开,再用文火熬煮120min后关火倒出,得第二次煎煮液;自来水的加入量为药渣重量的10倍;(3) Then add tap water to the medicinal dregs, bring to a boil with strong fire, then turn off the fire and pour it out after simmering for 120 minutes to obtain the second decoction; the amount of tap water added is 10 times the weight of medicinal dregs;

(4)把步骤(2)所得的第一次煎煮液和步骤(3)所得的第二次煎煮液合并,过滤,浓缩,得到浓缩药液;浓缩药液的密度为1.5g/cm3(4) The first decoction liquid of step (2) gained and the second decoction liquid of step (3) gained are combined, filtered and concentrated to obtain concentrated medicinal liquid; the density of concentrated medicinal liquid is 1.5g/cm 3 ;

(5)再把朴硝、雄黄粉及步骤(1)所得雷丸粉倒进浓缩药液中,搅拌均匀,即得本发明中药农药。(5) Pour the salted salt, realgar powder and thunder pill powder obtained in step (1) into the concentrated medicinal liquid, and stir evenly to obtain the traditional Chinese medicine pesticide of the present invention.

实施例3 Embodiment 3 :

一种中药农药,由按重量份比的以下原料制成:使君子60份、桑叶30份、岗松30份、臭椿叶20份、朴硝30份、大叶桉30份、满山香25份、洋金花10份、雄黄粉10份、五倍子20份、黑牵牛20份、鱼腥草20份和雷丸20份。A traditional Chinese medicine pesticide, which is made from the following raw materials in proportion by weight: 60 parts of Gentleman, 30 parts of mulberry leaves, 30 parts of Gangsong pine, 20 parts of Ailanthus ailanthus leaves, 30 parts of Pu Nitrate, 30 parts of Eucalyptus eucalyptus, 25 parts of Manshanxiang , 10 parts of Dajinhua, 10 parts of realgar powder, 20 parts of gallnut, 20 parts of black petunia, 20 parts of Houttuynia cordata and 20 parts of Lei Wan.

所述的中药农药的制备方法,包括以下步骤:The preparation method of described traditional Chinese medicine pesticide, comprises the following steps:

(1)按重量份数称取以上各中药原料,将雷丸干燥,打成细粉,得雷丸粉;雷丸粉的细度为120目;(1) take above each Chinese medicine raw material by parts by weight, dry the thunder pill, beat into fine powder, obtain the thunder pill powder; the fineness of the thunder pill powder is 120 orders;

(2)将使君子、桑叶、岗松、臭椿叶、大叶桉、满山香、洋金花、五倍子、黑牵牛、鱼腥草10种中药置入大瓦锅内,加入自来水,浸泡9h后,用武火烧开,再用文火熬煮80min后,过滤,将药液和药渣分离,得第一次煎煮液;自来水的加入量为10种中药重量的18倍;(2) Put 10 kinds of traditional Chinese medicines such as Shijunzi, mulberry leaves, pine pines, Ailanthus leaves, Eucalyptus euphratica, Manshanxiang, Yangjinhua, gallnut, petunias, and Houttuynia cordata into a large earthenware pot, add tap water, and soak After 9 hours, bring to a boil with a strong fire, then boil with a slow fire for 80 minutes, filter, separate the medicinal liquid and medicinal residues, and obtain the first decoction liquid; the amount of tap water added is 18 times the weight of 10 kinds of traditional Chinese medicines;

(3)然后往药渣中再加入自来水,用武火烧开,再用文火熬煮80min后关火倒出,得第二次煎煮液;自来水的加入量为药渣重量的8倍;(3) Then add tap water to the medicinal dregs, bring to a boil with strong fire, then turn off the heat and pour it out after simmering for 80 minutes to obtain the second decoction; the amount of tap water added is 8 times the weight of medicinal dregs;

(4)把步骤(2)所得的第一次煎煮液和步骤(3)所得的第二次煎煮液合并,过滤,浓缩,得到浓缩药液;浓缩药液的密度为1.3g/cm3(4) The first decoction liquid of step (2) gained and the second decoction liquid of step (3) gained are combined, filtered and concentrated to obtain concentrated medicinal liquid; the density of concentrated medicinal liquid is 1.3g/cm 3 ;

(5)再把朴硝、雄黄粉及步骤(1)所得雷丸粉倒进浓缩药液中,搅拌均匀,即得本发明中药农药。(5) Pour the salted salt, realgar powder and thunder pill powder obtained in step (1) into the concentrated medicinal liquid, and stir evenly to obtain the traditional Chinese medicine pesticide of the present invention.

实施例4:本发明的中药农药的杀虫效果 Embodiment 4 : the insecticidal effect of traditional Chinese medicine pesticide of the present invention

试验地点1:南宁市石埠镇安平村某香瓜田,面积3亩。 Test site 1 : a melon field in Anping Village, Shibu Town, Nanning City, with an area of 3 mu.

2015年6月,该田中的香瓜在刚刚开花时,发生了蚜虫、螨虫危害,导致香瓜叶片大面积发黄,并且香瓜株下部的叶片开始脱落。将这3亩香瓜划分为四个区域,A区按照常规方式喷洒化学农药敌敌畏,B、C、D区分别对应喷施实施例1、2、3的中药农药,喷施时将药液稀释10倍,喷施量以周到无滴落为准。In June 2015, when the melons in the field were just blooming, aphids and mites occurred, causing the leaves of the melons to turn yellow in large areas, and the leaves at the lower part of the melon plants began to fall off. These 3 acres of cantaloupe are divided into four areas, the A area sprays the chemical pesticide dichlorvos according to the conventional method, and the B, C, and D areas correspond to spraying the traditional Chinese medicine pesticides of embodiments 1, 2, and 3 respectively, and the medicinal liquid is diluted by 10% when spraying. times, the amount of spraying is subject to thoroughness and no dripping.

喷洒农药3日后对田内香瓜进行观察(详见表1),发现A区香瓜症状并无明显好转,而B、C、D区的香瓜苗则有变青趋势,病虫害得到了遏制,其中以D区情况最好;隔7天后又喷施1遍,3天后观察,发现A区香瓜病情并无并无明显缓解,而B、C、D区香瓜上则未发现有害虫,这说明原有蚜虫、螨虫已被杀灭或驱除,并且香瓜叶片明显变青,长势旺盛。After 3 days of spraying pesticides, the muskmelon in the field was observed (see Table 1 for details), and it was found that the symptoms of muskmelon in area A did not improve significantly, while the muskmelon seedlings in areas B, C, and D showed a tendency to turn green, and the pests and diseases were contained. The condition of the area was the best; after 7 days, it was sprayed again, and after 3 days of observation, it was found that the condition of the muskmelon in A area was not significantly relieved, while no harmful insects were found on the muskmelon in areas B, C, and D, which indicated that the original aphids 1. The mites have been killed or expelled, and the leaves of the muskmelon are obviously green and growing vigorously.

表1本发明的中药农药的防效The preventive effect of the traditional Chinese medicine pesticide of the present invention of table 1

处理deal with 蚜虫防效(%)Aphid control effect (%) 螨虫防效(%)Mite control effect (%) 长势growth AA 6060 5252 长势较差poor growth BB 8585 8686 长势旺盛Vigorous CC 8383 8181 长势旺盛Vigorous DD. 8080 8383 长势旺盛Vigorous

实施地点2:南宁市武鸣县太平镇林渌村某芥菜地,面积2亩。 Implementation site 2 : A mustard field in Linlu Village, Taiping Town, Wuming County, Nanning City, with an area of 2 mu.

2015年2月底,武鸣县太平镇林渌村某芥菜地发生了大面积菜青虫病害,严重影响了芥菜的品质。取实施例3的中药农药药液,稀释10倍喷施,三日后观察,未发现害虫,防效效果为100%。At the end of February 2015, a mustard field in Linlu Village, Taiping Town, Wuming County suffered a large area of mustard disease, seriously affecting the quality of mustard. Get the traditional Chinese medicine pesticide liquid of embodiment 3, dilute 10 times and spray, observe after three days, do not find pest, and control effect is 100%.

实施地点3:南宁市邕宁区广良村某番茄地,面积2亩。 Implementation site 3 : A tomato field in Guangliang Village, Suining District, Nanning City, with an area of 2 mu.

2015年5月中旬,地主人发现该番茄地发生了大面积蚜虫和螨虫,该番茄此时已进入结小花苞期。为了获得绿色无害的番茄产品,地主人求助于申请人。施以本发明实施例2的中药农药(药液稀释10倍),3日后,灭虫率达到92%以上,效果明显。尤其是,周边其他地里的害虫也没有向该地块蔓延,说明本发明的中药农药具有很好的驱虫效果。In mid-May 2015, the landowner discovered that aphids and mites had occurred in a large area in the tomato field, and the tomato had entered the stage of forming small flower buds. In order to obtain green and harmless tomato products, the landowner turned to the applicant. Apply the traditional Chinese medicine pesticide of the embodiment 2 of the present invention (dilution 10 times), after 3 days, the deinsectization rate reaches more than 92%, and the effect is obvious. In particular, the pests in other surrounding fields did not spread to the plot, indicating that the traditional Chinese medicine pesticide of the present invention has a good deworming effect.

实施地点4:百色市田东县麻疯村某黄瓜田,面积3亩。 Implementation site 4 : A cucumber field in Leprosy Village, Tiandong County, Baise City, with an area of 3 mu.

2014年5月,田东县麻疯村某黄瓜田黄瓜苗在开花前得了花叶病毒病,症状表现为:聚拢头,不生长。为对比用药效果,故将黄瓜田划分成了A、B、C、D四个小区,其中A区按照常规用量叶面喷施50%多菌灵WP 1000倍,B、C、D三个小区分别对应喷施实施例1、2、3的中药农药,叶面喷施,喷施时将药液稀释8倍,喷施量以周到无滴落为准。In May 2014, cucumber seedlings in a cucumber field in Leprosy Village, Tiandong County got mosaic virus disease before flowering. The symptoms were: gathered heads and no growth. In order to compare the drug effects, the cucumber field was divided into four plots A, B, C, and D. Among them, the A area was sprayed with 50% carbendazim WP 1000 times according to the conventional dosage, and the three plots B, C, and D Correspondingly spraying the traditional Chinese medicine pesticide of embodiment 1, 2, 3 respectively, foliar spraying, during spraying, medicinal liquid is diluted 8 times, and spraying amount is as the criterion with thoughtfulness without dripping.

3日后观察,详见表2,各小区黄瓜的花叶病毒病都得到了遏制,不再继续恶化,但是病毒病并没有完全消除;隔7天后再次用药,3日后观察病毒病完全消除。15天后发现,B、C、D三个小区的黄瓜长势明显好于A区黄瓜。Observe after 3 days, see Table 2 for details, the mosaic virus disease of cucumbers in each plot has been contained, no longer continue to deteriorate, but the virus disease has not been completely eliminated; medication again after every 7 days, and the virus disease was observed to be completely eliminated after 3 days. After 15 days, it was found that the growth of cucumbers in the three plots of B, C, and D was significantly better than that of the cucumbers in the A zone.

表2本发明的中药农药的防效The preventive effect of the traditional Chinese medicine pesticide of the present invention of table 2

同年,在当地还对茄子、土豆等蔬菜花叶病毒病的防治也进行了类似实验,同样获得了很好的防治效果。In the same year, similar experiments were also carried out locally on the prevention and control of vegetable mosaic virus diseases such as eggplant and potatoes, and good control effects were also obtained.

实施地点5:百色市田阳县那坡镇万平村某葡萄田,面积3亩。 Implementation site 5 : a grape field in Wanping Village, Napo Town, Tianyang County, Baise City, with an area of 3 mu.

2015年8月初,在百色市田阳县那坡镇万平村某葡萄田,在葡萄定植后选取四个小区做如下对比:A、B、C三个小区分别喷施实施例1-3的中药农药,药液稀释10倍后施用,喷施周到;D区以清水代替。At the beginning of August 2015, in a grape field in Wanping Village, Napo Town, Tianyang County, Baise City, after the grapes were planted, four plots were selected for comparison as follows: three plots A, B, and C were sprayed with the traditional Chinese medicine pesticides of Examples 1-3 respectively , Dilute the liquid medicine 10 times before applying, and spray thoroughly; D area is replaced with water.

施药3天后观察,发现在葡萄的整个生长期内,A、B、C三个小区的蚜虫发生率明显低于D区,3个月后收获时,A、B、C三个小区的葡萄较D区明显产量高、畸形率低。After 3 days of application, it was found that during the entire growth period of the grapes, the incidence of aphids in the three plots A, B, and C was significantly lower than that in the D plot. When harvesting after 3 months, the grapes in the three plots A, B, and C Compared with the D area, the yield is obviously higher and the deformity rate is lower.

表3本发明的中药农药的防效The preventive effect of the traditional Chinese medicine pesticide of the present invention of table 3

处理deal with 蚜虫防效(%)Aphid control effect (%) 长势growth AA 8080 长势旺盛Vigorous BB 8585 长势旺盛Vigorous CC 8383 长势旺盛Vigorous DD. 6060 长势较差poor growth

同样的,本发明的中药农药对于稻谷、冬瓜上的蚜虫、螨虫也具有很好的防治效果。Similarly, the traditional Chinese medicine pesticide of the present invention also has a good control effect on aphids and mites on rice and wax gourd.

前述对本发明的具体示例性实施方案的描述是为了说明和例证的目的。这些描述并非想将本发明限定为所公开的精确形式,并且很显然,根据上述教导,可以进行很多改变和变化。对示例性实施例进行选择和描述的目的在于解释本发明的特定原理及其实际应用,从而使得本领域的技术人员能够实现并利用本发明的各种不同的示例性实施方案以及各种不同的选择和改变。本发明的范围意在由权利要求书及其等同形式所限定。The foregoing descriptions of specific exemplary embodiments of the present invention have been presented for purposes of illustration and description. These descriptions are not intended to limit the invention to the precise form disclosed, and obviously many modifications and variations are possible in light of the above teaching. The exemplary embodiments were chosen and described in order to explain the specific principles of the invention and its practical application, thereby enabling others skilled in the art to make and use various exemplary embodiments of the invention, as well as various Choose and change. It is intended that the scope of the invention be defined by the claims and their equivalents.

Claims (7)

1. a Farm chemical of Chinese berbs, it is characterised in that be made up of following raw material by weight: Fructus Quisqualis 50-70 part, Folium Mori 20-40 part, Folium Baeckeae 25-35 part, ailanthus altissima (mill.) swingle leaf 15-25 part, Mirabilitum 20-35 part, Folium Eucalypti Robustae 25-35 part, MANSHANXIANG 20-30 part, ocean JINHUA 5-20 part, Realgar powder 5-15 part, Galla Chinensis 15-25 part, HEIQIANNIU 15-25 part, Herba Houttuyniae 15-30 part and Omphalia 15-30 Part.
Farm chemical of Chinese berbs the most according to claim 1, it is characterised in that be made up of following raw material by weight: make monarch Son 65 parts, 30 parts of Folium Mori, Folium Baeckeae 30 parts, 20 parts of ailanthus altissima (mill.) swingle leaf, Mirabilitum 30 parts, Folium Eucalypti Robustae 30 parts, MANSHANXIANG 25 parts, Flos Daturae 19 Part, Realgar powder 13 parts, Galla Chinensis 20 parts, HEIQIANNIU 20 parts, Herba Houttuyniae 25 parts and Omphalia 25 parts.
The preparation method of Farm chemical of Chinese berbs the most according to claim 1 and 2, it is characterised in that comprise the following steps:
(1) weigh above each raw material of Chinese medicine by weight, Omphalia is dried, breaks into fine powder, obtain Omphalia powder;
(2) by Fructus Quisqualis, Folium Mori, Folium Baeckeae, ailanthus altissima (mill.) swingle leaf, Folium Eucalypti Robustae, MANSHANXIANG, Flos Daturae, Galla Chinensis, HEIQIANNIU, Herba Houttuyniae 10 Kind of Chinese medicine is inserted in big tile pot, adds tap water, after soaking 8-10h, the most boiled, then with after slow fire infusion 60-90min, Filter, medicinal liquid is separated with medicinal residues, obtain decoction liquor for the first time;
(3) then in medicinal residues, tap water is added, the most boiled, then pour out with closing fire after slow fire infusion 60-120min, Decoction liquor for the second time;
(4) the first time decoction liquor of step (2) gained and the second time decoction liquor of step (3) gained are merged, filter, concentrate, Obtain concentrated medicament;
(5) again Mirabilitum, Realgar powder and step (1) gained Omphalia powder are poured in concentrated medicament, stir, obtain in the present invention Medicinal herb grower's medicine.
The preparation method of Farm chemical of Chinese berbs the most according to claim 3, it is characterised in that in step (1), Omphalia powder is thin Degree is 100-200 mesh.
The preparation method of Farm chemical of Chinese berbs the most according to claim 3, it is characterised in that in step (2), tap water adds Enter that amount is 10 kinds of Chinese medicine weight 15-20 times.
The preparation method of Farm chemical of Chinese berbs the most according to claim 3, it is characterised in that in step (3), tap water adds Enter that amount is medicinal residues weight 5-10 times.
The preparation method of Farm chemical of Chinese berbs the most according to claim 3, it is characterised in that concentrated medicament in step (4) Density is 1.0-1.5g/cm3
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CN106912506A (en) * 2017-03-09 2017-07-04 海门市嘉富来农产品有限公司 A kind of environment-friendly pesticide and preparation method thereof
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Application publication date: 20170111